US Patent 8168413 - Preparing luminescent nanodiamonds
http://www.freepatentsonline.com/8168413.html
This patent from Academia Sinica teaches luminescent nanodiamonds as an alternative to semiconductor nanocrystals for molecular biolabeling in order to avoid the toxicity of nanocrystals. Claim 1 reads:
1. A method of making luminescent diamond particles, comprising:
irradiating diamond particles with an ion beam, wherein the diamond particles have a diameter of 1 nm to 1 mm and 5 ppm to 1000 ppm color centers and the ion bean has a kinetic energy of 1 KeV to 900 MeV; and
heating the irradiated diamond particles in a non-oxidizing atmosphere at a temperature between 600 and 1000° C.; and
oxidizing the surface of the luminescent diamond particles.
This patent from Academia Sinica teaches luminescent nanodiamonds as an alternative to semiconductor nanocrystals for molecular biolabeling in order to avoid the toxicity of nanocrystals. Claim 1 reads:
1. A method of making luminescent diamond particles, comprising:
irradiating diamond particles with an ion beam, wherein the diamond particles have a diameter of 1 nm to 1 mm and 5 ppm to 1000 ppm color centers and the ion bean has a kinetic energy of 1 KeV to 900 MeV; and
heating the irradiated diamond particles in a non-oxidizing atmosphere at a temperature between 600 and 1000° C.; and
oxidizing the surface of the luminescent diamond particles.
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