US Patent 7569205 - Dispersion of nanodiamonds
http://www.freepatentsonline.com/7569205.html
Nanodiamonds have potential as additives to improve lubricants and for polishing. However, nanodiamonds can suffer from the same clumping problems of other nanomaterials. This patent teaches a processing method in which dimethyl sulfoxide is used to deaggregate the nanodiamonds. Claim 1 reads:
1. A method of processing detonation nanodiamonds to fractionate the detonation nanodiamonds comprising, in order:
providing detonation nanodiamonds,
forming a combination consisting essentially of said detonation nanodiamonds and a solvent, said nanodiamonds exhibiting a positive zeta potential in said solvent, said solvent consisting essentially of DMSO making up at least approximately 10% DMSO (v/v) in the solvent with any balance of the solvent consisting essentially of a polar solvent, wherein the DMSO increases or stabilizes the magnitude of the positive zeta potential of the detonation nanodiamonds in the combination,
applying a dispersive technique to said combination, subjecting said combination to a procedure that causes nanodiamond particles of a first size range to be substantially spatially separated from nanodiamonds of a second size range, and collecting said nanodiamonds of said first size range essentially free of said second size range.
Nanodiamonds have potential as additives to improve lubricants and for polishing. However, nanodiamonds can suffer from the same clumping problems of other nanomaterials. This patent teaches a processing method in which dimethyl sulfoxide is used to deaggregate the nanodiamonds. Claim 1 reads:
1. A method of processing detonation nanodiamonds to fractionate the detonation nanodiamonds comprising, in order:
providing detonation nanodiamonds,
forming a combination consisting essentially of said detonation nanodiamonds and a solvent, said nanodiamonds exhibiting a positive zeta potential in said solvent, said solvent consisting essentially of DMSO making up at least approximately 10% DMSO (v/v) in the solvent with any balance of the solvent consisting essentially of a polar solvent, wherein the DMSO increases or stabilizes the magnitude of the positive zeta potential of the detonation nanodiamonds in the combination,
applying a dispersive technique to said combination, subjecting said combination to a procedure that causes nanodiamond particles of a first size range to be substantially spatially separated from nanodiamonds of a second size range, and collecting said nanodiamonds of said first size range essentially free of said second size range.
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